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电化学(中英文) ›› 2008, Vol. 14 ›› Issue (2): 205-209.  doi: 10.61558/2993-074X.1892

• 研究论文 • 上一篇    下一篇

烧结温度对Ru-Ir-Sn氧化物阳极涂层性能的影响

嵇雷;王均涛;许立坤;刘文彬;薛桂林;   

  1. 哈尔滨工程大学材料科学与化学工程学院,海洋腐蚀与防护国家重点实验室中船重工725所青岛分部,海洋腐蚀与防护国家重点实验室中船重工725所青岛分部,哈尔滨工程大学材料科学与化学工程学院,哈尔滨工程大学材料科学与化学工程学院 黑龙江哈尔滨150001,海洋腐蚀与防护国家重点实验室,中船重工725所青岛分部,山东青岛266071,山东青岛266071,山东青岛266071,黑龙江哈尔滨150001,黑龙江哈尔滨150001
  • 收稿日期:2008-05-28 修回日期:2008-05-28 出版日期:2008-05-28 发布日期:2008-05-28

The Effect of Annealed Temperature On Properties of Ru-Ir-Sn Oxide Anode Coatings

JI Lei1,2,WANG Jun-tao2,XU Li-kun2,LIU Wen-bin1,XUE Gui-lin1,2   

  1. (1.Departement of Material Science and Chemical Enginering of Harbin Engineering University,Harbin 150001,China;2.State Key Laboratory for Marine Corrosion and Protection,Qingdao Branch of Luoyang Ship Material Research Institute,Qingdao 266071,Shandong,China
  • Received:2008-05-28 Revised:2008-05-28 Published:2008-05-28 Online:2008-05-28

摘要: 应用溶胶凝胶法制备不同焙烧温度的氧化物阳极涂层,SEM,EDX,XRD、强化电解寿命、循环伏安和电化学阻抗等测试表明,烧结温度对阳极涂层的表面形貌以及电化学性能有着很大的影响.随着烧结温度的升高,析氯电位相应增加,寿命相对较长,循环伏安电量与双电层电容值有所下降.

关键词: 氧化物阳极涂层, 焙烧温度, 溶胶凝胶

Abstract: The anode coatings of Ru-Ir-Sn oxide were prepared by sol-gel method with different annealed temperatures.The influences of annealed temperature in properties of anode coatings were characterized by scanning electron microscope(SEM),energy dispersive X-ray detector(EDX),X-ray diffraction(XRD),potential of chlorine evolution,accelerated life,cyclic voltammetry and electrochemical impedance spectroscopy(EIS) tests.The results showed that the annealed temperature affected the morphology of coatings,while the electric quantities of cyclic voltammetry and double layer capacitances of anode coatings had a tendency to fall down and the potential of chlorine evolution and accelerated life had a tendency to increase as the annealed temperature increased.

Key words: oxide anode coatings, annealed temperature, solgel

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