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研究论文

XYZ-2型高性能电化学离子色谱抑制柱

  • 胡维玲
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  • 厦门大学固体表面物理化学国家重点实验室厦门大学物理化学研究所厦门大学化学系

收稿日期: 1999-05-28

  修回日期: 1999-05-28

  网络出版日期: 1999-05-28

XYZ_2 High_Performance Electrochemical Suppressorfor Ion Chromatography

  • Hu WeilingLin Huashui
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  • (Dept. of Chem.Xiaman Univ., Xiaman 361005

Received date: 1999-05-28

  Revised date: 1999-05-28

  Online published: 1999-05-28

摘要

本文研究离子色谱电化学抑制器的填料问题,提出以直径大小一致、中等磺化深度的球状树脂为最佳方案.改进后的抑制效率达99.98%,灵敏度提高了约10%,离子的峰高及保留时间的重现性均优良(c.v.<2).

关键词: 离子色谱; 电导; 抑制器

本文引用格式

胡维玲 . XYZ-2型高性能电化学离子色谱抑制柱[J]. 电化学, 1999 , 5(2) : 212 -217 . DOI: 10.61558/2993-074X.3178

Abstract

The packings of electrochemical suppressor on ion chromatography were studied,It was found that the best packing is the appropriately sulfonate globular resins uniform in size.Using these resins,suppression efficiency was improved to 99.98%,and sensitivity improves about 10%,the reproducibilities of both the height of ion peaks and retention time are very good(c.v<2).

参考文献

1ZWTian,RZHu,HSLin,JTWu.High_performanceelectrochemicalsuppresorforionchromatography.J.Chromatograph.,1988,439:159~1632StevensTS,DavisJC,SmalH.HolowFiberion_exchangesuppresorforionchromatography.Anal.Chem.,1981,53:1488~14923HanaokaY,MurayamaT,MuramotoS,MatsuraT,HanbaA.Ionchromatographywithanion_exchangemembranesuppressor.Chromatogr.,1982,239:537~5484FranklinGO.DevelopmentandapplictionsofionchromategraphyAm.Lab.(Fairfield,conn.),1985
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