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研究论文

电化学法制备Zn-Ni合金晶须

  • 梁镇海 ,
  • 夏玺华
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  • 太原理工大学化学化工学院,太原理工大学化学化工学院 山西太原030024,山西太原030024

收稿日期: 2008-05-28

  修回日期: 2008-05-28

  网络出版日期: 2008-05-28

Preparation of Zn-Ni Alloy Whisker by Electrochemical Method

  • LIANG Zhen-hai ,
  • XIA Xi-hua
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  • (College of Chemistry and Chemical Engineering,Taiyuan University ofTechnology,Taiyuan 030024,Shanxi,China

Received date: 2008-05-28

  Revised date: 2008-05-28

  Online published: 2008-05-28

摘要

应用电化学方法制备Zn-Ni合金晶须.样品的成分、形貌用XRD、SEM、EDS等方法表征,结果表明,晶须的物相是Ni5Zn21和Ni3Zn22,直径250 nm,长度2~4μm,长径比8~16.同时用循环伏安法探讨了该过程的电化学行为.为晶须的制备提供了一种新的方法.

关键词: Ni5Zn21; Ni3Zn22; 晶须; 电化学

本文引用格式

梁镇海 , 夏玺华 . 电化学法制备Zn-Ni合金晶须[J]. 电化学, 2008 , 14(2) : 180 -183 . DOI: 10.61558/2993-074X.1887

Abstract

The Zn-Ni alloy whiskers were prepared by electrochemical method and were characterized by XRD、SEM and EDS methods.The results showed that Ni5Zn21 and Ni3Zn22 whiskers were obtained with the length of 2~4 μm and the diameter of 250 nm,thereby the rations of length/diameter fell between 8 and 16.The electrochemical behavior was investigated by cyclic voltammetry method simultaneously.A new method was provided on whisker preparation based on this work.
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