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原位57Fe穆斯堡尔光谱技术及其在Ni-Fe基析氧反应电催化剂中的应用
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In-Situ/Operando 57Fe Mössbauer Spectroscopic Technique and Its Applications in NiFe-based Electrocatalysts for Oxygen Evolution Reaction
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Figure 5. CVs of NiFe layered oxyhydroxide (blue) and hydrous Fe oxide (green) electrocatalysts used for the in-situ/operando experiments with 57Fe Mössbauer spectra collected at open circuit potential (gray), 1.49 V(purple), 1.62 V(yellow), and 1.76 V(red) vs. RHE. CV data were recorded in the Mössbauer-electrochemical cell with a scan rate of 25 mV·s-1 prior to Mössbauer measurements[ |
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