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原位57Fe穆斯堡尔光谱技术及其在Ni-Fe基析氧反应电催化剂中的应用
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In-Situ/Operando 57Fe Mössbauer Spectroscopic Technique and Its Applications in NiFe-based Electrocatalysts for Oxygen Evolution Reaction
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Figure 3. Cyclic voltammograms were taken during the aging of films in various purities of KOH. A total of 13 CV scans are shown for each sample: one for the initial as-deposited film (the dark purple), and one additional scan after each 5 min aging period up to a total of 1 hour of aging (the dark red). The changes in the anodic and cathodic peak positions (ΔEp,a and ΔEp,c) are labeled for each set of CVs. (ΔEp,a value is shown for the Ni0.75Fe0.25(OH)2, as the oxidation peak is partially obscured by the OER current.)[ |
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